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- W1993116883 abstract "High-resolution atomic force microscopy (AFM) of polymers requires the surface of specimens to be relatively-flat, ordered, and rigid. Crystalline polymers can provide such samples in the form of solution-grown single crystals and melt-drawn films. Images of surfaces of solution-grown single crystals of alkanes showed a lattice of chain ends, whereas the surface of longer alkanes of hydroxybutyrate showed evidence of chain folding. Highly-oriented, melt-spun films of poly(ethylene) exhibited a shish-kebab structure. Molecular resolution images of the lamellar crystals were obtained and steps <1 nm high in the surface were attributed to slip traces. Similarly prepared films of poly(butene-1) (PB-1) only consisted of extended-chain needle crystals with no lamellar overgrowth. In molecular resolution images, the pitch of the molecules was similar to the X-ray diffraction value, and the ethyl side groups appeared to have rearranged on the surface compared to the bulk structure. In an investigation of tin graphoepitaxy on PB-1, contact mode AFM swept away the tin particles, whereas with tapping mode the particles remained stationary on the surface." @default.
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- W1993116883 date "1994-08-01" @default.
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- W1993116883 title "Atomic force microscopy of polymer single crystals and melt-drawn films" @default.
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- W1993116883 doi "https://doi.org/10.1016/0927-7757(94)80071-5" @default.
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