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- W1993350003 abstract "The preparation of packed capillaries with stable frits of good quality can be a hurdle to obtain efficient separations in capillary electrochromatography (CEC). Especially with particles smaller than 3 μm, frit preparation is cumbersome. Highly efficient separations using packed capillaries without frits are presented. Under appropriate CEC conditions the particles were retained by electrophoretic attraction towards the anode by a tapered capillary inlet, without the need of a frit at the outlet end. Such fritless capillaries, packed with 1.5 μm nonporous reversed-phase particles, allowed separations with efficiencies of more than 500 000 plates/m. Once the capillaries were conditioned properly, more than 100 separations could be performed with good repeatability. With respect to separation efficiency, fritless capillaries packed with 3 μm particles were comparable with standard CEC capillaries with frits. Examples of separations of steroids, a pesticide and its by-products, and cardiac glycosides under various CEC conditions are shown." @default.
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- W1993350003 date "1999-01-01" @default.
- W1993350003 modified "2023-09-25" @default.
- W1993350003 title "Fritless capillary electrochromatography" @default.
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- W1993350003 doi "https://doi.org/10.1002/(sici)1522-2683(19990101)20:1<43::aid-elps43>3.0.co;2-8" @default.
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