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- W1993481041 abstract "A method for the determination of acenocoumarol in human plasma by capillary gas chromatography—mass-selective detection is described. After addition of a structurally related analogue as the internal standard, the compounds are extracted from plasma at acidic pH into toluene, back-extracted with a basic solution and re-extracted from hydrochloric acid solution with toluene, which is then evaporated to dryness. The compounds are converted into their methyl derivatives, which are determined by gas chromatography using a mass-selective detector at m/z 324 for acenocoumarol and m/z 338 for the internal standard. The reproducibility and accuracy of the method were found to be suitable over the acenocoumarol concentrations range 2.2–74 nmol/l. The method could be considered as selective for acenocoumarol in the presence of its major metabolites in plasma." @default.
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- W1993481041 title "Determination of acenocoumarol in human plasma by capillary gas chromatography with mass-selective detection" @default.
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- W1993481041 doi "https://doi.org/10.1016/0378-4347(93)e0434-r" @default.
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