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• W1993574080 abstract "We show for the first time that it is possible to acquire high-resolution heteronuclear NMR correlation experiments in solid state between second-order-broadened half integer quadrupolar nuclei (i.e., 27Al and 17O) using the scalar J-coupling. The sensitivity of the experiment is dramatically improved at high fields (gain proportional to the fourth power of the principal field) with a combination of signal enhancement techniques. This turns a challenging experiment into a real tool. We apply this experiment to characterize a calcium aluminate glass in which we prove the presence of tricluster mu3 oxygen sites and describe the signature of their directly bonded aluminum sites. Applications involve a large range of possible pairs of quadrupolar nuclei in different materials, such as glasses, porous or mesoporous framework materials, zeolites, hybrid organic-inorganic, and bioinvolved materials." @default.
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• W1993574080 date "2005-07-27" @default.
• W1993574080 modified "2023-10-16" @default.
• W1993574080 title "NMR Heteronuclear Correlation between Quadrupolar Nuclei in Solids" @default.
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• W1993574080 doi "https://doi.org/10.1021/ja052452n" @default.
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