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- W1993853516 abstract "Polysulfonylamines. CLXXVIII. Onium Salts of Benzene-1,2-di(sulfonyl)amine (HZ): A Second Crystal Form of the Ammonium Salt NH4Z·H2O and Crystal Structure of the Bis(triphenylphosphoranylidene)ammonium Salt [Ph3PNPPh3]Z A dimorphic form of NH4Z·H2O, where Z− is N-deprotonated ortho-benzenedisulfonimide, has been obtained and structurally characterized (previously known form 1A: monoclinic, P21/c, Z′ = 1; new polymorph 1B: monoclinic, P21/n, Z′ = 1). Both structures are dominated by an abundance of classical hydrogen bonds N+–H/O–H···O=S/OH2, whereby the anionic N− function does not act as an acceptor. The major difference between the dimorphs arises from the topology of the hydrogen bond network, which is two-dimensional in 1A, leading to a packing of discrete lamellar layers, but three-dimensional in 1B. Moreover, the latter network is reinforced by a set of weak C–H··O/N hydrogen bonds, whereas the layered structure of 1A displays only one independent C–H···O bond, providing a link between adjacent layers. The compound [Ph3PNPPh3]Z (2, monoclinic, P21/c, Z′ = 1) is the first structurally authenticated example of an ionic Z− derivative in which the cation contains neither metal bonding sites nor strong hydrogen bond donors. This structure exhibits columns of anions, surrounded by four parallel columns of cations, giving a square array. The large cations are associated into a three-dimensional framework via weak C–H···C(π) interactions and an offset face-to-face phenyl interaction, while the anions occupy tunnels in this framework and are extensively bonded to the surrounding cations by C–H···O/N− hydrogen bonds and C–H···C(π) interactions." @default.
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- W1993853516 date "2007-04-01" @default.
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- W1993853516 title "Polysulfonylamine. CLXXVIII Onium-Salze des Benzol-1,2-di(sulfonyl)amins (HZ): Eine zweite Kristallform des Ammonium-Salzes NH4Z·H2O und Kristallstruktur des Bis(triphenylphosphoranyliden)ammonium-Salzes [Ph3PNPPh3]Z" @default.
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- W1993853516 doi "https://doi.org/10.1002/zaac.200600352" @default.
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