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• W1993856013 abstract "The thermal behaviour of pure basic nickel carbonate, ammonium molybdate and their mixtures in different ratios were studied by means of TG, DTG, and DTA analyses. Relative thermal analysis (RTA) graphical treatment of derivatographic curves of the components in the pure and binary system has been carried out. X-ray diffraction (XRD) analysis and infrared (IR) spectroscopy were used to characterize the solids produced from thermal treatment at temperature ranges between 250 and 1000 °C. The results obtained revealed that pure nickel carbonate decomposed into NiO at 250 °C, while pure ammonium molybdate decomposed into MoO3 at 340 °C and then melted at 790 °C. Crystalline (NH4)4Mo8O26 and (NH4)4Ni4(NH3)3Mo5O20 phases were detected for mixtures precalcined at 250 °C. For the binary components, crystalline nickel or molybdenum oxides were detected beside nickel molybdate phase starting from 500 °C. The latter phase was formed as a result of solid–solid interaction and its formation is exothermic in character. The calcination temperature and composition of the mixture directly affect the formation of NiMoO4 phase. The compound formed is thermally stable up to 1000 °C. The presence of two-component solids in the binary systems affected the thermal decomposition of their individual salt and affected their physical and chemical behaviour." @default.
• W1993856013 created "2016-06-24" @default.
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• W1993856013 date "2002-02-01" @default.
• W1993856013 modified "2023-09-23" @default.
• W1993856013 title "Thermal behaviour of pure and binary basic nickel carbonate and ammonium molybdate systems" @default.
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• W1993856013 doi "https://doi.org/10.1016/s0167-577x(01)00406-2" @default.
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