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- W1994293801 abstract "Poly-L-lactide (PLLA) having two anthracene (diene) terminals and poly-D-lactide (PDLA) having two maleimide (dienophile) termainals were prepared by the ordinary ring-opening polymerization (ROP) of L- and D-lactides with the corresponding functional initiators followed by the coupling reaction of the resultant terminal hydroxyls of the PLLA and PDLA prepolymers with hexamethylene diisocyanate (HMDI), respectively. The di-functional PLLA and PDLA obtained were then mixed and subjected to Diels–Alder coupling to spontaneously form PLLA-PDLA stereo multiblock copolymers (m-sb-PLA: PLLA-multi-PDLA) whose block sequences could readily be controlled by changing the molecular weight of the PLLA and PDLA prepolymers first synthesized by the ROP. The finally chain-extended m-sb-PLAs were found to have excellent thermal stability and thermo-mechanical properties because of the easy formation of stereocomplex crystals of PLLA and PDLA by retaining high molecular weight. This synthetic method based on the dual terminal couplings can afford a convenient route to stereo block copolymers of PLLA and PDLA having excellent properties and processability." @default.
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- W1994293801 date "2012-12-01" @default.
- W1994293801 modified "2023-10-02" @default.
- W1994293801 title "Synthesis of stereo multiblock polylactides by dual terminal couplings of poly-L-lactide and poly-D-lactide prepolymers: A new route to high-performance polylactides" @default.
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- W1994293801 doi "https://doi.org/10.1016/j.polymer.2012.10.051" @default.
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