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- W1994513986 abstract "Abstract Esterification of hemicelluloses of the xylan family was performed in order to produce hydrophobic films. Acylation reactions were carried out with lauroyl chloride in the N,N-dimethylacetamide/lithium chloride homogeneous system using 4-dimethylaminopyridine as activator and were induced by microwave irradiation. In the experimental conditions used, 108 and 172% mass ratios were obtained for the dodecyl-grafted xylan and heteroxylan, respectively. The degrees of substitution (DS) were 1.3 (maximum 2) for xylan and 1.2 (maximum 2.1) for heteroxylan. These products were further characterized by FT-IR spectroscopy. The mechanical and thermomechanical behavior of this new family of hydrophobic films were analyzed and compared to those obtained from cellulose with a similar DS by the means of tensile tests. Our results indicate that the dodecyl-grafted xylan film presents the best rigidity—resistance to traction ratio." @default.
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- W1994513986 date "2004-01-01" @default.
- W1994513986 modified "2023-09-27" @default.
- W1994513986 title "Chemical Valorization of Forest and Agricultural By-Products. Obtention, Chemical Characteristics, and Mechanical Behavior of a Novel Family of Hydrophobic Films" @default.
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- W1994513986 doi "https://doi.org/10.1081/pfc-200026884" @default.
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