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- W1994595036 abstract "An efficient and convenient procedure for the synthesis of estriol 16- and 17-monoglucuronides from estriol is described. This is achieved by the selective protection and deprotection of the hydroxy groups in estriol, Koenigs-Knorr reactions with methyl 1-bromo-1-deoxy-2,3,4-tri-O-acetyl -α- d - glucopyranuronate and subsequent hydrolysis. The products have been characterised by proton nuclear magnetic resonance ( 1 H NMR), two-dimensional 1 H homonuclear shift-correlated spectra (2D-COSY) and mass spectra. The selective Koenigs-Knorr reaction of the alcoholic hydroxyl group in the presence of a phenolic hydroxyl group is also reported ." @default.
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- W1994595036 date "1993-10-01" @default.
- W1994595036 modified "2023-09-27" @default.
- W1994595036 title "The synthesis of estriol 16- and 17-monoglucuronide from estriol" @default.
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- W1994595036 doi "https://doi.org/10.1016/0039-128x(93)90001-4" @default.
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