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• W1994602724 abstract "The effect of mass transfer on the electropolishing of nickel in sulphuric acid solutions has been studied using a rotating disc electrode technique. Two well defined regions for different rotation rates have been observed having (a) pure diffusion control, and (b) mixed kinetic and diffusion control. The presence of a solid layer of a hydrated nickel salt covering a contaminated oxide layer is proposed. The rate of chemical attack of the underlying layer appears to depend on the SO2−4 ion concentration for H2SO4 concentrations greater than 8 M. When the rate of mass transfer is increased, changes in the morphology of the surface are observed, polishing gives way to levelling, and finally either to metallographic etching or corrosion. The disappearance of electropolishing is observed in general when the rate of mass transfer is sufficient to eliminate from the surface the solid layer of hydrated nickel sulphate, and the results indicate a coupling between diffusional rates in the solution and ionic transport through the oxide or contaminated oxide phases." @default.
• W1994602724 created "2016-06-24" @default.
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• W1994602724 date "1982-07-01" @default.
• W1994602724 modified "2023-09-27" @default.
• W1994602724 title "The influence of mass transfer on the mechanism of electropolishing of nickel in aqueous sulphuric acid" @default.
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• W1994602724 doi "https://doi.org/10.1016/0013-4686(82)80205-3" @default.
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