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- W1994631323 abstract "Two gas-tight cells with appropriate electrodes were constructed of transparent polypropylene and kept at constant temperature in a water bath. Simultaneous measurements of pH, conductivity and temperature as a function of time were carried out in the first cell containing a solution with the molar ratio (TMOS:H2O:HCl) of 1:4:10−3 or 1:4:10−4. The H+ ion limiting current was periodically determined by linear voltammetry on a Pt microelectrode in the second cell with the same solution. The measurement were made in deoxygenated solutions, at 25°C , 40°C or 50°C and extended to a point after gelation until the contact between the respective electrode and the gel broke down. A significant temperature change was found to occur in the first 20 min after mixing. Strong fluctuations of pH and conductivity were observed in this period. The subsequent changes with time of temperature, pH, conductivity and limiting current were small. The results are discussed in relation to other studies." @default.
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- W1994631323 date "1997-08-01" @default.
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- W1994631323 title "Studies of changes of pH, H+ ion limiting current, conductivity and temperature during sol-gel processes in a TMOS system" @default.
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- W1994631323 doi "https://doi.org/10.1016/s0022-0728(97)00189-7" @default.
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