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- W1994646687 abstract "(CH3)4N+SO2CN- was prepared from (CH3)4N+CN- and SO2 and characterized by 1H, 13C, 14N NMR, infrared, and Raman spectroscopy. The yellow salt is stable up to −10 °C, but solutions in SO2 decompose already at −50 °C in 1 day. The structure of the anion was predicted by ab initio calculations, suggesting Cs symmetry with a pyramidal coordination at the central sulfur atom with the following geometry: d(SO) = 146.7 pm, d(SC) = 190.8 pm, ∠(OSO) = 114.0°, ∠(OSC) = 100.8°, and ∠(SCN) = 173.6°. The bent SCN arrangement is explained by negative hyperconjugation." @default.
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- W1994646687 date "1999-04-01" @default.
- W1994646687 modified "2023-09-25" @default.
- W1994646687 title "Synthesis and Characterization of Tetramethylammonium Cyanosulfite, (CH3)4N+SO2CN-" @default.
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- W1994646687 doi "https://doi.org/10.1021/ja9833422" @default.
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