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- W1994738449 abstract "The reaction between Ni[Salen] (Salen bis(salicylaldehyde)ethylenediiminato) and Zn(C2H5)2 in hydrocarbon solvents yields the Ni[Salen]·Zn(C2H5)2 adduct. An X-ray crystal structure (monoclinic, space group P21/c, a 12.835(5), b 14.072(11), c 13.766(8) Å, β 117.48(5)°, V 2206(5) Å3, Z = 4) shows that the Zn atom is surprisingly weakly coordinated to the cis oxygen atoms of the Salen ligand. The averagen ZnO distance is 2.321(6) Å leading to an acute OZnO angle of 63.1(2)°. The CZn angle of 147.9(4)° is also indicative of a relative weak interaction of the Zn with the Salen oxygen atoms. The Zn atom is displaced 0.78 Å from the least-squares plane of the Ni coordination plane. There were no chemically significant changes in the coordination parameters of Ni[Salen] on adduct formation. Attempts to form adducts with other related systems are discussed." @default.
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- W1994738449 date "1988-11-01" @default.
- W1994738449 modified "2023-10-12" @default.
- W1994738449 title "Bimetallic metal alkyl systems; synthesis and characterization of the Ni[Salen]·Zn(C2H5)2 adduct" @default.
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- W1994738449 doi "https://doi.org/10.1016/0022-328x(88)83095-x" @default.
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