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- W1994797297 abstract "The planar dihydroxo-bridged [Cu2(dpyam)2(μ-OH)2I2] · 2H2O (1) and the roof-shaped trihydroxo-bridged [Cu2(dpyam)2(μ-OH)3]Cl · 3H2O (2) (in which dpyam = di-2-pyridylamine) dinuclear copper(II) compounds have been synthesized and their crystal structures determined by X-ray crystallographic methods. All of compounds are being centrosymmetric molecule. Compound 1 contains a dinuclear [I(dpyam)Cu(μ-OH)2Cu(dpyam)I]+ unit with a strictly planar CuO2 network, dihedral angle between the CuO2 planes of 180°. Each copper(II) ion is in a tetrahedrally distorted square pyramidal coordination geometry of the CuN2O2I chromophore with a dihedral angle 19.3° between the CuN2 and CuO2 planes. In the dinuclear [(dpyam)Cu(μ-OH)3Cu(dpyam)]+ unit of compound 2, the triply bridged Cu(II) ions show a distorted square pyramidal coordination. The fifth apical ligand is a longer bonded bridging OH− group, at distance of 2.433(4) Å, which joins the basal CuN2O2 planes in a roof-shaped configuration with a dihedral angle of 142.5°. The Cu–Cu distance is 2.803(7) Å." @default.
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- W1994797297 date "2004-05-01" @default.
- W1994797297 modified "2023-10-16" @default.
- W1994797297 title "The novel dinuclear doubly and triply bridged copper(II) compound with monoatomic bridges" @default.
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- W1994797297 doi "https://doi.org/10.1016/j.poly.2004.03.021" @default.
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