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- W1994840610 abstract "The new polymer poly(thiophene-2,5-diyl-1,2-dimethoxyvinylene) was synthesized by a benzoin condensation of thiophene-2,5-dicarboxaldehyde to poly(2,5-thienylene-1-oxo-2-hydroxyethylene) (Mw ∼ 1 × 106, pd ∼ 13), followed by O-alkylation using dimethyl sulfate. A side reaction of the benzoin condensation step leading to dimethyl-2,5-thiophenedicarboxylate can be avoided by using cyclohexanol as the solvent. The O-alkylation, including the workup, has to be performed under nitrogen protection to counteract the degradation of the polymer by air under the influence of light. A mechanism is proposed for the oxidative degradation of this poly(thiophene-2,5-diylvinylene) derivative and other poly(arylenevinylenes). Conductivity and thermal properties of the new polymer are given." @default.
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- W1994840610 date "1996-01-01" @default.
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- W1994840610 title "Synthesis, Characterization, and Stability of High Molecular Weight Poly(thiophene-2,5-diyl-1,2-dimethoxyvinylene)" @default.
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- W1994840610 doi "https://doi.org/10.1021/ma951106v" @default.
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