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• W1995072013 abstract "Abstract A gold polycrystalline electrode modified with rhodium species was characterized by electrochemical and XPS (X-ray photoelectron spectroscopy) techniques in moderately alkaline medium. The Au/Rh electrodes were prepared utilizing a spontaneous deposition process (SDP) of rhodium adlayer on the gold surface. In particular, rhodium deposition was obtained in non-deaerated 50 mM HClO 4 solution containing 10 mM RhCl 3 at open circuit for a given time. The modified gold electrode with adsorbed rhodium species (Au/Rh) exhibit higher electrochemical activity for the oxygen evolution reaction. The effects on the electrochemical activity of the Au/Rh electrode such as: rhodium coverage, pH, electrolyte composition and applied potentials were critically evaluated and discussed. An optimized pulsed chronoamperometric detection technique for the analytical determination of several mono- and di-protic organic acids such as acetic, tartaric, oxalic, malic, etc., was successfully proposed. An average film composition of Au 93±1 Rh 7±1 was evaluated by XPS technique. The film composition remains unchanged after various electrode treatments such as cycling of potentials and/or polarization conditions for long times in alkaline medium. Thus, the adsorbed rhodium oxide particles show a good chemical and mechanical stability despite the conditions of electrochemical treatment of the electrode surface." @default.
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• W1995072013 creator A5021314257 @default.
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• W1995072013 date "2007-08-01" @default.
• W1995072013 modified "2023-09-25" @default.
• W1995072013 title "Rhodium-modified gold polycrystalline surface as anode material in alkaline medium: An electrochemical and XPS investigation" @default.
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• W1995072013 doi "https://doi.org/10.1016/j.jelechem.2007.04.009" @default.
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