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- W1995149382 abstract "Dynamic viscoelastic properties of poly(vinyl chloride) (PVC)/bis(2-ethylhexyl) phthalate (DOP) gels with different molecular weights and various polymer concentrations have been studied as a function of temperature. These PVC gels exhibited an elastic solid at room temperature and gradually became liquid (sol) with increasing temperature. The sol−gel transition took place at a critical gel temperature at which the scaling law of G‘(ω) ∼ G‘‘(ω) ∝ ωn held, allowing an accurate determination of the critical gel temperature by means of the frequency independence of the loss tangent. The scaling exponent n obtained was 0.75, independent of temperature as well as molecular weight. This is in good agreement with the previous results observed at 40 °C and suggests the formation of a similar fractal structure of the PVC gels. Furthermore, the molecular structure of the gel junctions was analyzed using the modified Eldridge−Ferry procedure developed by Tanaka and Nishinari. The junction structure was found to be almost independent of molecular weight and gelation temperature, giving a support to the similarity of the fractal structure in the PVC gels." @default.
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- W1995149382 date "1998-10-20" @default.
- W1995149382 modified "2023-10-07" @default.
- W1995149382 title "Rheological Images of Poly(vinyl chloride) Gels. 6. Effect of Temperature" @default.
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- W1995149382 doi "https://doi.org/10.1021/ma980556v" @default.
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