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• W1995343868 abstract "Abstract Preliminary results of Raman spectroscopy are presented on “in situ” growth of carbon nanotubes in a CVD‐cell which is optionally coupled to a mass spectrometer (MS). The system allows to analyze the differences in the content of the types of carbon nanotubes in the sample during the processes after 2 min, 5 min, 10 min, 15 min, 20 min and 30 min. The evolved gases in the throughout synthesis were analyzed in the MS mode. Two kinds of experiments were performed: in argon atmosphere at atmospheric pressure and under vacuum at low pressure, both with CH 4 as a carbon feedstock. The temperature of the experiments was set up to 600 °C. The detailed study of the process can lead to a better understanding of the carbon nanotube growth mechanism. The analysis of these phenomena is supported by high resolution transmission electron microscopy (HR‐TEM). In addition, thermogravimetric analyses of the finally obtained products in the two experiments are presented. (© 2008 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
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• W1995343868 date "2008-09-24" @default.
• W1995343868 modified "2023-10-17" @default.
• W1995343868 title "“In situ” observations of carbon nanotube generation in CVD cell coupled to spectrometers" @default.
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• W1995343868 doi "https://doi.org/10.1002/pssb.200779629" @default.
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