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- W1995355243 abstract "2-O-Methanesulfonyl-β-D-mannose was reacted with kryptofix/K2CO3/[18F]fluoride in CH3CN/THF (9:1) at 60°C. Unexpectedly, a mixture of 1α- and 1β-glucopyranosyl [18F]fluoride (4 and 5, respectively) was obtained in 50% radiochemical yield (EOB); 2-[18F]FDG was not detected. Modification of temperature, solvent or pH did not result in the formation of 2-[18F]FDG. Uptake of radioactivity in heart and brain of mice was significantly lower for 4 and 5 than for 2-[18F]FDG, although 5 seems to pass the blood-barrier. Uptake in bone was more pronounced for 4 than for 5 and negligible for 2-[18F]FDG. Copyright © 1999 John Wiley & Sons, Ltd." @default.
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- W1995355243 date "1999-02-01" @default.
- W1995355243 modified "2023-09-24" @default.
- W1995355243 title "Synthesis of 1-[18F]fluorodeoxyglucose: an unexpected rearrangement in the reaction of 2-O-methanesulfonyl-β-D-mannopyranose with [18f] fluoride" @default.
- W1995355243 doi "https://doi.org/10.1002/(sici)1099-1344(199902)42:2<147::aid-jlcr176>3.0.co;2-e" @default.
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