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- W1995385620 abstract "The title compound Cu2(fsa)2en, CH3OH was synthesized and its crystal structure solved at room temperature from 3830 independent reflections. It crystallizes in the monoclinic system, space group P21/n. The lattice constants are a = 11.456(5) Å, b = 11.425(3) Å, c = 14.357(4) Å and β = 104.15(3)° with Z = 4. Least squares refinement of the structure led to a conventional weighted R factor of 0.043. The structure is made of non-symmetrical binuclear units in which a copper atom is five-fold coordinated to two nitrogens, two phenolic oxygens and an oxygen of the methanol molecule, the other copper atom being coordinated to two phenolic oxygens and two carboxylic oxygens in a plannar manner. The temperature dependence of the magnetic susceptibility, studied in the range 10–312 K, showed a strong antiferromagnetic coupling with a J singlet-triplet separation of −650 cm−1. This magnetic behaviour was compared to those of the other binuclear complexes with the same Cu2O2 network and an explanation for such a strong coupling was proposed." @default.
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- W1995385620 date "1979-01-01" @default.
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- W1995385620 title "Crystal structure and magnetic properties of Cu2(fsa)2en, CH3OH, with H4(fsa)2en = N,N′-bis(2-hydroxy, 3-carboxybenzilidene)-1,2-diaminoethane" @default.
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- W1995385620 doi "https://doi.org/10.1016/s0020-1693(00)89398-6" @default.
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