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- W1995651110 abstract "The change of electrodeposited manganese oxide on gold during the reduction process was investigated in borate solution at pH 9.2, using in situ optical techniques. Raman spectroscopy (RS) showed five bands of manganese dioxide at 410, 480, 520, 580 and 640 cm−1, which decreased and disappeared during the cathodic discharge process. These changes occurred reversibly during the reduction-oxidation cycle. The band at 580cm−1 can be assigned to the MnO stretching because of the correlation found between the XPS analyses and the Raman spectroscopy. In situ Raman spectra of thermal manganese oxide were also performed, and showed the same five Raman bands at 415, 485, 515, 585 and 635cm−1. Electrochemically modulated infrared spectroscopy (EMIRS) is associated with the appearance of a OH stretching band. The changes of RS, EMIRS and XPS reveal the proton—electron injection for the reduction reaction of electrolytic MnO2." @default.
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- W1995651110 date "1993-02-01" @default.
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- W1995651110 title "A study of the discharge process of manganese oxide in borate solution using in situ techniques" @default.
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- W1995651110 doi "https://doi.org/10.1016/0013-4686(93)85149-s" @default.
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