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- W1995657312 abstract "Eine neue, ergiebige Methode zur Herstellung der isomeren 1.3.5-Triamino-cyclohexane, ausgehend von 1.3.5-Trinitro-benzol, wird beschrieben. Durch Kondensation von 1.3.5-Tris-propionylamino-cyclohexan (5) und 1.3.5-Tris-benzolsulfonylamino-cyclohexan (8) mit Orthoameisensäure-triäthylester sind N.N′.N”︁-Tripropionyl- (6) und N.N′.N”︁-Tris-benzol-sulfonyl-2.4.10-triaza-adamantan (9) zugänglich. Die analoge Reaktion von N-Methyl-benzolsulfonamid mit Orthoameisensäureester führt dagegen zu äthoxy-bis-[N-methylbenzolsulfonylamino]-methan (10). Compounds with Urotropin Structure, XLV Cyclisations Starting from 1,3,5-Triaminocyclohexane A new method for preparation in good yield of the isomeric 1,3,5-triaminocyclohexanes starting from 1,3,5-trinitrobenzene is reported. N, N′,N″-Tripropionyl-2,4,10-triazaadamantane (6) and N, N′,N″-tris(benzenesulfonyl)-2,4,10-triazaadamantane (9) could be obtained by condensation of l,3,5-tris(propionylamino)cyclohexane (5) and l,3,5-tris(benzenesulfonamido)cyclohexane (8) with triethyl orthoformiate. On the other hand, condensation of N-methyl-benzenesulfonamide with triethyl orthoformiate leads to ethoxy-bis(N-methylbenzenesulfonamido)methane (10)." @default.
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- W1995657312 date "1970-01-01" @default.
- W1995657312 modified "2023-10-17" @default.
- W1995657312 title "Über Verbindungen mit Urotropin‐Struktur, XLV Cyclisierungsreaktionen ausgehend von 1.3.5‐Triamino‐cyclohexan" @default.
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- W1995657312 doi "https://doi.org/10.1002/cber.19701030127" @default.
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