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- W1996004865 abstract "Bis(trimethylsilyl)cyclopentadiene reacts with two equivalents of boron halides to the bis(dihalogenoboryl)cyclopentadienes I, II and III. Reactions of I, II and III with tetramethyltin and dimethylamine yield the dimethyl- and bis(dimethylamino)-substituted compounds IV and V. The fluoro compound VI is synthesized by the reaction of III with arsenic trifluoride. Addition of pyridine to I and II yields the adducts VII and VIII. Structure and bonding properties of I–VIII are discussed by 1H-, 13C-, 11B- and 19F.n.m.r- and by i.r. and m.s. data. Bis(trimethylsilyl)cyclopentadien reagiert mit zwei Äquivalenten Bortrihalogenid zu den Bis(dihalogenoboryl)cyclopentaidenen I, II und III. Reaktionen von I, II und III mit Zinntetramethyl und Dimethylamin führen zu den dimethyl- und bis(dimethylamino)-substituierten Verbindungen IV und V. Die Fluorverbindung VI wird durch Umsetzung von III mit Arsentrifluorid dargestellt. Zugabe von Pyridin zu I und II führt zu den addukten VII and VIII. Struktur und Bindungsverhältnisse von I–VIII werden anhand von 1H-, 13C-, 11B- und 19F-NMR- und von IR- und MS-Daten diskutiert." @default.
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- W1996004865 date "1979-04-01" @default.
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- W1996004865 title "Synthese und Struktur von 1.4-Diborylcyclopentadienen" @default.
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- W1996004865 doi "https://doi.org/10.1016/s0022-328x(00)80975-4" @default.
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