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• W1996304328 endingPage "3060" @default.
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• W1996304328 abstract "Two new one-dimensional organic/inorganic composite polymers were synthesized by the reaction of Cd(NO3)2·4H2O with 1,2-bis(4-pyridyl)ethyne or trans-1,2-bis(4-pyridyl)ethene in several solvent systems. [Cd(NO3)2(1,2-bis(4-pyridyl)ethyne)1.5]n (1), which has an infinite one-dimensional structure with interpenetrating molecular ladders, was obtained by reacting Cd(NO3)2·4H2O with 1,2-bis(4-pyridyl)ethyne in a methylene chloride/methanol solvent system. It crystallized in the monoclinic space group C2/c (No. 15), with a = 20.713(3) Å, b = 17.450(2) Å, c = 14.451(3) Å, β = 129.203(8)°, Z = 8. [Cd(NO3)2(1,2-bis(4-pyridyl)ethene)1.5]n (2) was generated from the reaction of Cd(NO3)2·4H2O with the trans-1,2-bis(4-pyridyl)ethene ligand in an ethanol/water system. It has a novel infinite non-interpenetrating zigzag chain structure which is made up of trans-1,2-bis(4-pyridyl)ethene−Cd−trans-1,2-bis(4-pyridyl)ethene−Cd−trans-1,2-bis(4-pyridyl)ethene building units. Compound 2 crystallized in the triclinic space group P1̄ (No. 2), with a = 10.725(2) Å, b = 10.814(2) Å, c = 9.517(2) Å, α = 104.21(2)°, β = 94.60(1)°, γ = 106.62(1)°, Z = 2. In compound 1, the Cd(II) centers lie in a heptacoordinate environment, while in compound 2, the Cd(II) atoms adopt an octahedral geometry. The two kinds of polymer structures are based on a T-shape and a linear building block, respectively. [Cd(NO3)2(1,2-bis(4-pyridyl)ethane)1.5]n (3) was also synthesized by the reaction of Cd(NO3)2·4H2O with the 1,2-bis(4-pyridyl)ethane ligand in a methylene chloride/methanol system. Polymer 3 forms square units, which are linked through the two Cd(II) centers to give infinite linear chains. The synthesis of compound 3 was reported by Fujita (Fujita, M. J. Chem. Soc., Chem. Commun. 1994, 1977) using a different solvent system." @default.
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• W1996304328 date "1999-05-29" @default.
• W1996304328 modified "2023-09-23" @default.
• W1996304328 title "Syntheses and Characterizations of One-Dimensional Coordination Polymers Generated from Cadmium Nitrate and Bipyridine Ligands" @default.
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• W1996304328 doi "https://doi.org/10.1021/ic9814569" @default.
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