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- W1996423114 abstract "Abstract Two types of intermetallic lithium alloys, Li 21 Si 5 and Li 17 Sn 4 (previously Li 22 Si 5 and Li 22 Sn 5 ), were prepared for the first time using microwave-assisted solid-state reaction. The optimum oven power for their preparation is 80–60%, and the irradiation times are 5 min for Li 21 Si 5 or 10 min for Li 17 Sn 4 . A cheap alumina crucible was found to be the most suitable container in quick (less than 10 min) microwave reactions for Li-containing alloys. The synthesized compounds were characterized by PXRD. Mossbauer spectroscopy was used to characterize Li 17 Sn 4 under different conditions. The hyperfine interaction parameters of 119 Sn in Li 17 Sn 4 show a typical Li–Sn alloy Sn isomer shift (1.88 mm/s). The oxidization processes of the two intermetallic lithium alloys in air were investigated. The microwave method was found to be simple, fast and efficient, with high selectivity for the preparation of these compounds." @default.
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- W1996423114 date "2004-09-01" @default.
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- W1996423114 title "Microwave-assisted selective preparation and characterization of Li21Si5 and Li17Sn4" @default.
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- W1996423114 doi "https://doi.org/10.1016/j.jssc.2004.04.045" @default.
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