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- W1996493791 abstract "Arsenic(III) can be amperometrically detected by oxidation at a platinum or gold electrode in perchloric acid solutions. Platinum is the preferred material because halides interfere with the oxidation of arsenic(III) at gold electrodes. The limiting current for arsenic(III) at the platinum electrode is less than the value predicted for a mass transport limited reaction. This decrease results either from slow linear diffusion of arsenic(III) through the oxide film, or from cylindrical diffusion to widely dispersed active sites on an inhomogeneous electrode surface. The anodic current for arsenic(III) is reproducible when the oxide film reaches a constant thickness. The detection limit for a platinum-wire flow-through detector is approximately 0.4 ppb arsenic(III). Arsenic(V) is determined after reduction to arsenic(III) by hydrazine sulfate. A cation-exchange column in the flow analyzer prevents interference from excess of hydrazine." @default.
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- W1996493791 title "Anodic detection of arsenic(III) in a flow-through platinum electrode for flow-injection analysis" @default.
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- W1996493791 doi "https://doi.org/10.1016/s0003-2670(01)84312-9" @default.
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