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• W1996562045 abstract "Homonuclear Hartmann–Hahn transfer is one of the most important building blocks in modern high-resolution NMR. It constitutes a very efficient transfer element for the assignment of proteins, nucleic acids, and oligosaccharides. Nevertheless, in macromolecules exceeding ∼10 kDa TOCSY-experiments can show decreasing sensitivity due to fast transverse relaxation processes that are active during the mixing periods. In this article we propose the MOCCA-XY16 multiple pulse sequence, originally developed for efficient TOCSY transfer through residual dipolar couplings, as a homonuclear Hartmann–Hahn sequence with improved relaxation properties. A theoretical analysis of the coherence transfer via scalar couplings and its relaxation behavior as well as experimental transfer curves for MOCCA-XY16 relative to the well-characterized DIPSI-2 multiple pulse sequence are given." @default.
• W1996562045 created "2016-06-24" @default.
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• W1996562045 date "2004-01-01" @default.
• W1996562045 modified "2023-10-11" @default.
• W1996562045 title "Homonuclear Hartmann–Hahn transfer with reduced relaxation losses by use of the MOCCA-XY16 multiple pulse sequence" @default.
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• W1996562045 doi "https://doi.org/10.1016/j.jmr.2003.09.013" @default.
• W1996562045 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/14675818" @default.
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