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- W1996567175 abstract "Tris(3-thiocyanato-2,4-pentanediono) FeIII, bis(3-thiocyanato-2,4-pentanediono) PdII, tris(2-thiocyanato-1-phenyl-1,3-butanediono) CrIII, tris(2-thiocyanato-1,3-diphenyl-1,3-propanediono) CrIII, tris(2-thiocyanato-1-phenyl-1,3-butanediono) CoIII and tris(2-thiocyanato-1,3-diphenyl-1,3-propanediono) CoIII have been prepared by the thiocyanation of corresponding metal 1,3-diketonates with thiocyanogen. Possible mechanism of thiocyanation has been outlined. Rates of reactions and relative yields have been discussed in terms of principal steric and electronic effects of the substituents in the chelate rings. Dibenzoylmethane has been found to replace acetylacetone from the labile metal acetylacetonates providing a method for the preparation of metal dibenzoylmethanates. Infrared and electronic spectral data have been recorded and are discussed." @default.
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- W1996567175 date "1968-03-01" @default.
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- W1996567175 title "Chemical and spectroscopic studies in metal β-diketonates. IV. Simpler preparations of metal 1,3-diketonates and their thiocyanation" @default.
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- W1996567175 doi "https://doi.org/10.1016/s0020-1693(00)87004-8" @default.
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