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- W1996631402 abstract "Thermal decomposition of [NMe4]2[V2O2F6(H2O)2] has been investigated by simultaneous TG, DTG and DTA. Measurements have been carried out in a dynamic atmosphere of dry air and argon, respectively. Intermediate phases and final products have been characterized by X-ray powder and infrared spectroscopy. Thermal decomposition in argon is accomplished in three steps. In the first water is given off, the second and the third ones, however, overlap, and the stoichiometries of the decomposition reactions are not evident from the TG curve. The final product is an impure vanadium trifluoride. Thermal decomposition in air also gives anhydrous compound in the first step. Further pyrolysis is entirely different due to oxidation of tetramethylammonium and of vanadium. The final product of the decomposition is vanadium pentoxide." @default.
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- W1996631402 date "1987-05-01" @default.
- W1996631402 modified "2023-09-26" @default.
- W1996631402 title "Thermal decomposition of tetramethylammonium di-μ-fluorobis[aquadifluoro-oxovanadate(IV)]" @default.
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- W1996631402 doi "https://doi.org/10.1016/0040-6031(87)88371-5" @default.
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