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Matches in SemOpenAlex for { <https://semopenalex.org/work/W1996808846> ?p ?o ?g. }

• W1996808846 abstract "Radiolabelled raloxifene (LY156758) has been prepared by tritium gas hydrogenolysis of a 3-aroyl-bis-brominated precursor. The requisite halogenated intermediate was accessed by regioselective aroylation of benzothiophene 6 with the acid chloride of 3,5-dibromo-4-[2-(1-piperdinyl)ethoxy]benzoic acid (5). Selective deprotection of the aryl methyl ethers in the presence of the ethoxy side-chain followed by palladium catalyzed halogen-tritium exchange provided the target compound with a specific activity of 30.1 Ci/mmol." @default.
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• W1996808846 date "1995-01-01" @default.
• W1996808846 modified "2023-09-27" @default.
• W1996808846 title "A chemical probe for the estrogen receptor: Synthesis of the 3H-isotopomer of raloxifene" @default.
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• W1996808846 doi "https://doi.org/10.1002/jlcr.2580360105" @default.
• W1996808846 hasPublicationYear "1995" @default.
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