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- W1996968301 abstract "The ESR techniques were used in order to examine the presence of the radical species in the alkaline sulfide reduction of aromatic nitro compounds and in the photooxidation of an aqueous monosulfide solution. The ESR spectra were clear when observed by ultraviolet-light irradiation on an aqueous monosulfide solution: they were the signals of a singlet, with a g-value of 2.002±0.001 and a maximum slope width of 3.1 gauss, and a doublet, with a g-value of 2.00±0.001 and a coupling constant of 114 gauss. The singlet was identified as the signal of the sulfide ion radical, S·−, while it was most reasonable to assume the doublet to be signals due to the interaction of the sulfide ion radical with the hydrosulfide or the hydroxide in the solution. On the other hand, ESR spectra were also observed in the reaction of sodium m-nitrobenzene sulfonate with an aqueous monosulfide solution; these spectra were identical with the sulfide ion radical and the radical-anion of the nitro compound. On the basis of the results obtained, we have discussed the mechanisms of the alkaline sulfide reduction of aromatic nitro compounds and these reduction intermediates." @default.
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- W1996968301 date "1967-12-01" @default.
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- W1996968301 title "The Alkaline Sulfide Reduction of Aromatic Nitro Compounds. XII. ESR Studies of the Alkaline Sulfide Reduction of the Aromatic Nitro Compound" @default.
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- W1996968301 doi "https://doi.org/10.1246/bcsj.40.2867" @default.
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