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• W1997054483 abstract "The structure of the intermediate range order (IRO) of sodium borate glasses and melts were quantitatively investigated by the analysis of high-temperature Raman scattering spectra. Raman bands at the middle frequency region of 700–950 cm−1 were normalized using the bands at high frequency spectra and their intensities were compared among the spectra collected from the melts with different composition at various temperature. Bands at 805, 780, 750 and 720 cm−1 were focused and their intensity changes were quantified. The exceeds of temperature over the glass transition temperature did not necessarily cause the decrease of all the band intensities. At Na2O<15 mol%, 805 cm−1 band was the most sensitive to temperature, while at 15<Na2O<30, it was switched to 780 cm−1 band and 805 cm−1 band became insensitive. When Na2O concentration exceeded 30 mol%, 750 and 720 cm−1 bands were decreased with temperature. Accompanying the previous analysis on the structures of short range-order (SRO) of boron atoms [J. Non-Cryst. Solids, in this issue], some models of the structural rearrangement along with temperature were proposed. The combination of the obtained structural informations of IRO and SRO was found to explain the mechanisms causing various characteristic properties of borate glasses and melts, especially immiscibility and boron oxide anomaly of thermal expansion coefficient from the microscopic and dynamic points of view of the vitrification process in melt." @default.
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• W1997054483 date "2003-07-01" @default.
• W1997054483 modified "2023-10-18" @default.
• W1997054483 title "Structural investigation of sodium borate glasses and melts by Raman spectroscopy. III. Relation between the rearrangement of super-structures and the properties of glass" @default.
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• W1997054483 doi "https://doi.org/10.1016/s0022-3093(03)00160-1" @default.
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