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• W1997112963 abstract "Two different spectrofluorimetric methods for the determination of piroxicam (PX) in serum are presented and discussed. One of them is based on the use of three-way fluorescence data and multivariate calibration performed with parallel factor analysis (PARAFAC) and self-weighted alternating trilinear decomposition (SWATLD). This methodology exploits the so-called second-order advantage of the three-way data, allowing to obtain the concentration of the studied analyte in the presence of any number of uncalibrated (serum) components. The method was developed following two different procedures: internal standard addition and external calibration with standard solutions, which were compared and discussed. The second approach investigated is based on the combination of solid-phase extraction (SPE) and room temperature fluorimetry. Both methods here presented yield satisfactory results. The concentration range in which PX could be determined in serum was 1-10 microg ml(-1). The limits of quantification for the experimental solutions using the chemometric approach were 0.09 microg ml(-1) for the standard addition mode and 0.12 microg ml(-1) using external calibration (both for PARAFAC and SWATLD algorithms). In the solid-surface fluorimetric method, the calibration graph was linear up to 0.22 microg ml(-1) and the limit of quantification was 0.02 microg ml(-1)." @default.
• W1997112963 created "2016-06-24" @default.
• W1997112963 creator A5068327143 @default.
• W1997112963 date "2003-08-29" @default.
• W1997112963 modified "2023-10-03" @default.
• W1997112963 title "Two different strategies for the fluorimetric determination of piroxicam in serum" @default.
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• W1997112963 doi "https://doi.org/10.1016/s0039-9140(03)00221-2" @default.
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