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- W1997163366 abstract "The determination of tetracyclines (TC) in aqueous solutions, based on europium-sensitized fluorescence, has been improved using EDTA as co-ligand and cetyltrimethylammonium chloride as surfactant. The method involves working in slightly alkaline solutions with the formation of a new chelate where the lanthanide ion is bound to the β-diketone group. The method is about 6 times more sensitive than that with the Eu–TC–Triton system and LODs are 2.5 × 10−10, 5 × 10−10, 1.5 × 10−9 and 2 × 10−9 mol l−1 for TC, oxytetracycline, chlortetracycline and doxycycline, respectively. The method has been applied to the determination of TC in calf serum without sample pretreatment. The mean recovery was close to 102% and the lowest concentration attainable in serum samples was better than 0.1 μg ml−1." @default.
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- W1997163366 date "2001-01-01" @default.
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- W1997163366 title "Sensitive detection of tetracyclines using europium-sensitized fluorescence with EDTA as co-ligand and cetyltrimethylammonium chloride as surfactant" @default.
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- W1997163366 doi "https://doi.org/10.1039/b101525g" @default.
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