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- W1997223451 abstract "Abstract The synthesis, characterisation and catalytic behaviour of palladium compound derived from Mg/Al hydrotalcite were investigated in the toluene total oxidation. The hydrotalcite sample was prepared by co-precipitation of the corresponding chlorides (MgCl2, AlCl3 and H2PdCl4) with boiled fresh water and under N2 atmosphere. Under these conditions, the layered double hydroxide [Mg0.75Al0.25(OH)2]0.25+ PdCl 2 (OH) 2 0.125−x 2 − (CO3)x2−·nH2O was formed. Palladium species were inserted as [PdCl2(OH)2]2− complex coming from the partial substitution of Cl with OH. The space interlayer was imposed by CO32− present also as balancing anion. This new hydrotalcite is less stable than classical hydrotalcite Mg/Al without Pd since its destruction took place at a lower temperature. The palladium hydrotalcite calcined at 290 °C exhibited the best catalytic behaviour (activity and selectivity) in the total oxidation of toluene compared with a conventional palladium catalyst." @default.
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- W1997223451 date "2002-08-01" @default.
- W1997223451 modified "2023-10-16" @default.
- W1997223451 title "Characterisation of Mg/Al hydrotalcite with interlayer palladium complex for catalytic oxidation of toluene" @default.
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- W1997223451 doi "https://doi.org/10.1016/s0926-860x(02)00201-6" @default.
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