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- W1997331502 abstract "Reaction of [Pt(PEt3)X2]2 (X = Cl, Br) with two equivalents of K[H2B(pz)2] (pz = pyrazolyl ring) yields [η2-H2B(pz)2]Pt(PEt3)X contaminated with an impurity from which it could not be separated. A similar reaction with K[B(pz)4] (X = Br) yields the five-coordinate complex [η3-B(pz)4]Pt(PEt3)Br. In contrast, the K[HB(pz)3] ligand produces the unusual bridged dimer Br(PEt3)Pt{μ-[(pz)2BH(pz)]}Pt(PEt3)Br2. This complex forms in better yield in the stoichiometric reaction of one equivalent of the ligand per dimer. It has been characterized in the solid state by X-ray crystallography: orthorhombic, in the space group P212121 with a = 12.462(3), b = 30.985(5), c = 8.383(2) Å, V = 3237 Å3 and Z = 4. The complexes [MeC(O)CHC(O)Me]Pt(PEt3)Cl and [EtOCS2]Pt(PEt3)Cl have also been prepared from the reaction of [Pt(PEt3)Cl2]2 and the respective ligand salt." @default.
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- W1997331502 date "1989-11-01" @default.
- W1997331502 modified "2023-10-03" @default.
- W1997331502 title "Polypyrazolylborate-phosphine complexes of platinum(II). X-ray crystal structure of the unusual dimer Br(PEt3)Pt{μ-[(pz)2BH(pz)]}Pt(PEt3)Br2" @default.
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- W1997331502 doi "https://doi.org/10.1016/s0020-1693(00)83240-5" @default.
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