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- W1997580319 abstract "Using a thick-walled glass reaction vessel a number of transition-metal organometallic and co-ordination compounds have been synthesised using microwave dielectric super-heating effects. Super-heating by 40–60 °C is maintained by controlling the pressure at 10 atm and results in a decrease in the reaction time required for conventional reflux reactions by a factor of ca. 102. Full details of the design of the apparatus, the modification of a conventional microwave oven and the electrical circuitry for the pressure control are provided." @default.
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- W1997580319 date "1992-01-01" @default.
- W1997580319 modified "2023-09-23" @default.
- W1997580319 title "A new reaction vessel for accelerated syntheses using microwave dielectric super-heating effects" @default.
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- W1997580319 doi "https://doi.org/10.1039/dt9920001151" @default.
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