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• W1997652272 startingPage "3695" @default.
• W1997652272 abstract "Nanostructured vanadia model catalysts, i.e., highly dispersed vanadium oxide supported on mesoporous silica SBA-15 (VOx/SBA-15), were prepared. The mechanism for the synthesis of VOx/SBA-15 was elucidated by detailed characterization of the individual synthesis steps using XPS and vibrational spectroscopy. The resulting surface vanadium oxide species (0–2.3 V/nm2), grafted on the inner pores of the SBA-15 silica matrix, consists of tetrahedrally coordinated vanadia as inferred from UV–VIS- and Raman spectroscopy. The prepared vanadia model catalysts were tested in the partial oxidation of methanol to formaldehyde yielding high formaldehyde selectivities of 94% at 350 °C. XPS and Raman analysis of the catalyst after reaction reveal the presence of methoxy as well as a significant amount of carbonaceous species on the surface. Our results demonstrate that a detailed understanding of partial oxidation reactions requires the combination of complementary spectroscopic techniques ultimately within one experimental set-up." @default.
• W1997652272 created "2016-06-24" @default.
• W1997652272 creator A5028546703 @default.
• W1997652272 date "2006-09-01" @default.
• W1997652272 modified "2023-09-27" @default.
• W1997652272 title "Characterization of the synthesis and reactivity behavior of nanostructured vanadia model catalysts using XPS and vibrational spectroscopy" @default.
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• W1997652272 doi "https://doi.org/10.1016/j.susc.2005.11.063" @default.
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