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- W1997750185 abstract "Abstract An efficient synthetic method was developed for l -β-3′- C -cyano-2′,3′-unsaturated nucleosides and l -3′- C -cyano-3′-deoxyribonucleosides. The key intermediate 11 was obtained from l -xylose, from which a series of pyrimidine and purine nucleosides were prepared in high yield by the coupling of 11 and various silyl-protected bases in the presence of TMSOTf. These nucleosides were eliminated, followed by deprotecting to give l -β-3′- C -cyano-2′,3′-unsaturated nucleosides. When selectively deprotected by hydrazine hydrate in buffered acetic acid–pyridine followed by treatment with potassium carbonate in methanol, l -3′- C -cyano-3′-deoxyribonucleosides were obtained. The synthesized nucleosides were tested for anti-HIV activity." @default.
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- W1997750185 date "2003-12-16" @default.
- W1997750185 modified "2023-09-23" @default.
- W1997750185 title "Synthesis and anti-HIV Activity of L-β-3′-C-Cyano-2′,3′-unsaturated Nucleosides and L-3′-C-Cyano-3′-deoxyribonucleosides." @default.
- W1997750185 cites W2949211878 @default.
- W1997750185 doi "https://doi.org/10.1002/chin.200350208" @default.
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