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- W1998005248 abstract "Abstract The complexes [TpRuCl(dippe)] (dippe=1,2-bis(diisopropylphosphino)ethane) and [TpRuCl(PEt3)2] react with HNCPh2 and NaBPh4 in MeOH affording the cationic mononuclear imine derivatives [TpRu(HNCPh2)(dippe)][BPh4] and [TpRu(HNCPh2)(PEt3)2][BPh4], respectively. The X-ray crystal structure of the latter has been determined. The reaction of [TpRuCl(PMeiPr2)(MeCN)] with HNCPh2 led to the neutral imine derivative [TpRuCl(PMeiPr2)(HNCPh2)], which adds a second imine ligand upon chloride dissociation affording the cationic bis(imine) complex [TpRu(PMeiPr2)(HNCPh2)2]+. The cationic complexes [TpRu(HNCPh2)(dippe)][BPh4] and [TpRu(HNCPh2)(PEt3)2][BPh4] react with KOBut in tetrahydrofuran yielding the neutral metalated species [TpRu(σ-η1-C6H4C(Ph)NH)(dippe)] and the phenyl complex [TpRu(σ-η1-C6H5)(PEt3)2], respectively. All compounds were characterized by IR, NMR and microanalysis." @default.
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- W1998005248 date "2000-04-01" @default.
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- W1998005248 title "Synthesis and properties of hydrotris(pyrazolyl)borate (Tp) ruthenium complexes with benzophenone imine: X-ray crystal structure of [TpRu(HN=CPh2)(PEt3)2][BPh4]" @default.
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- W1998005248 doi "https://doi.org/10.1016/s0020-1693(00)00002-5" @default.
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