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- W1998032705 abstract "The divergent synthesis of novel phosphorus-containing dendrimer with 4,4'-sulphonyldiphenol at the core has been accomplished involving simple condensation reactions using <TEX>$P(O)Cl_3$</TEX>, <TEX>$P(S)Cl_3$</TEX>, 3-amino-phenol, 3-hydroxy-benzaldehyde, and 2-butyn 1, 4-diol. The final compound was a Schiff's base macromolecule possessing 4 imine bonds, 8 acetylenic bonds and 8 OH groups at the periphery. The structures of intermediate compounds were confirmed by IR, NMR (<TEX>$^1H$</TEX>, <TEX>$^{13}C$</TEX> and <TEX>$^{31}P$</TEX>), LC-Mass and C, H, N analysis. The structure of the final dendrimer (5) was confirmed by IR, NMR (<TEX>$^1H$</TEX>, <TEX>$^{13}C$</TEX> and <TEX>$^{31}P$</TEX>), MALDI-TOF-MS, and C, H, N analysis. The surface morphological characteristics of the final dendrimer were understood by Scanning Electronic Microscopic study (SEM). The thermal stability of the final dendrimer was studied by TGA/DTA analysis." @default.
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- W1998032705 date "2011-02-20" @default.
- W1998032705 modified "2023-09-26" @default.
- W1998032705 title "Synthesis, Spectral Characterization, Electron Microscopic Study and Influence on the Thermal Stability of Phosphorus-containing Dendrimer with a 4,4'-Sulphonyldiphenol at the Core" @default.
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- W1998032705 doi "https://doi.org/10.5012/bkcs.2011.32.2.498" @default.
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