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- W1998045993 abstract "The copolymerizations of allyl methacrylate (AMA) with methyl methacrylate (MMA) and of AMA with N-vinyl-2-pyrrolidone (VP) have been effected in bulk by γ-irradiation to various stages of fractional conversion θ extending over a wide span of θ. Addition of n-heptane isolated the crosslinked copolymer. FT i.r. analysis on the supernatant solution yielded the composition of unreacted monomer mixture, which was used in conjunction with θ and the composition of initial feed to determine the reactivity ratios (r) via an iterative procedure involving a simplex algorithm, yielding AMA(1)MMA(2) r1 = 1.55 ± 0.16, r2 = 0.99 ± 0.19 and AMA(1)VP(2) r1 = 1.408 ± 0.074, r2 = 0.401 ± 0.044. For the system AMAVP, analysis of crosslinked copolymer (via nitrogen analysis) was also possible and manipulation of the data by three modern procedures afforded good agreement with the values of r1 and r2 obtained by analysis of monomer mixture alone." @default.
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- W1998045993 date "1996-04-01" @default.
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- W1998045993 title "Reactivity ratios in copolymerizations involving allyl methacrylate" @default.
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- W1998045993 doi "https://doi.org/10.1016/0032-3861(96)81142-6" @default.
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