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- W1998069948 abstract "The lithium complexes RP(3,5- t Bu 2 C 6 H 2 OLi) 2 (THF) 4 , where R = Ph or i Pr, ( R [OPO]Li 2 ) 2 (THF) 4 , can be converted quantitatively into the protonated forms, R [OPO]H 2 , by reaction with Et 3 NHCl. Reaction of the protonated compounds with KH yields the potassium complexes ( Ph [OPO]K 2 ) 2 (THF) 6 and ( i Pr [OPO]K 2 ) 3 (THF) 3 . The reaction of R [OPO]H 2 with TaCl 5 yields the sparingly soluble tantalum trichloride complexes R [OPO]TaCl 3 via elimination of HCl. Reaction of Ph [OPO]H 2 with TaMe 3 Cl 2 leads to the monomethyl complex Ph [OPO]TaMeCl 2 , or the dimethyl halide complex, Ph [OPO]TaMe 2 Cl, via protonolysis, and the potassium complex ( Ph [OPO]K 2 ) 2 (THF) 6 yields the trimethyl complex, Ph [OPO]TaMe 3 by a metathesis process." @default.
- W1998069948 created "2016-06-24" @default.
- W1998069948 creator A5026785398 @default.
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- W1998069948 date "2010-07-01" @default.
- W1998069948 modified "2023-10-07" @default.
- W1998069948 title "<i>Ortho</i>-phenylene-bridged aryloxy phosphine ligands and their coordination chemistry with tantalum(V)" @default.
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- W1998069948 doi "https://doi.org/10.1139/v10-050" @default.
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