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- W1998136908 abstract "Self-assembly of AgX (X-=ClO4-,BF4-) with a new diethylbis(4-pyridyl)silane (L) ligand basically gives rise to a one-dimensional (1D) sinusoidal structure. Weak C–H⋯π interactions between ethyl and pyridyl groups result in the formation of infinite square supra-channel structures via a molecular array of four sinusoidal chains. The supra-channel size is 10.1–10.7 Å with a void cross-section of 2.1–3.1 Å for [Ag(L)](ClO4) and 9.9–10.5 Å with a void cross-section of 2.0–3.0 Å for [Ag(L)](BF4). The supra-channels are occupied by each counteranion. Anion exchange of [Ag(L)](BF4) with NaClO4 occurs smoothly, whereas the reverse anion exchange of [Ag(L)](ClO4) with NaBF4 does not. Calcination of [Ag(L)](ClO4) crystals at 400 °C produces a circle morphology with evolving burned organics, and, at 600 °C, forms network circles consisting of a silver(0)/silver chloride (chlorargyrite)/silicon(IV) oxide composite with a micro-sized convexo-concave surface. In contrast, calcination of [Ag(L)](BF4) crystals at 600 °C produces silver(0) materials without silicon(IV) oxide." @default.
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- W1998136908 date "2013-12-01" @default.
- W1998136908 modified "2023-10-16" @default.
- W1998136908 title "Subtle anion effects on anion exchange and thermolysis: Square supra-channels via array of sinusoidal coordination polymers" @default.
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- W1998136908 doi "https://doi.org/10.1016/j.molstruc.2013.09.056" @default.
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