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• W1998281154 endingPage "2377" @default.
• W1998281154 startingPage "2372" @default.
• W1998281154 abstract "A new methodology for the fabrication of covalently bound multilayers has been developed on the basis of a self-assembled monolayer (SAM) prepared from 5-(2-methyl-1,3,2-dioxaborinan-5-yl)pentyltrichlorosilane (1). The SAM was prepared by immersion of an aluminized silicon wafer into a toluene solution of 1; its thickness was determined by ellipsometry to be 1.5 ± 0.3 nm, a value very similar to the molecular size of 1. The fabrication of a two-layer film was successfully achieved by hydrolysis of the boronate protecting group of the SAM with water/ethanol to the diol-terminated group followed by treatment of the hydrolyzed monolayer with a toluene solution of 1; the thickness (2.9 ± 0.3 nm) was nearly twice that of the starting monolayer. Similar treatment of the two-layer film with water/ethanol effected the selective hydrolysis of the boronate end group without significant loss of the second-layer unit, and subsequent reactions of the hydrolyzed two-layer film with 1 or octadecyltrichlorosilane smoothly occurred to give the corresponding three-layer assembly with thickness of 4.2 ± 0.4 or 5.4 ± 0.5 nm each." @default.
• W1998281154 created "2016-06-24" @default.
• W1998281154 creator A5027410727 @default.
• W1998281154 creator A5088524416 @default.
• W1998281154 date "1998-04-01" @default.
• W1998281154 modified "2023-10-11" @default.
• W1998281154 title "Fabrication of Multilayer Assemblies Based on a Boronate-Terminated Self-Assembled Monolayer" @default.
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• W1998281154 doi "https://doi.org/10.1021/la971215y" @default.
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