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- W1998377589 abstract "A stereodivergent approach to creation of a specific 14-membered macrolide library is described. We designed a new 14-membered macrolide template possessing 10 sterogenic centers, and established a new library of fully-synthesized 14-membered ring compounds. The designed macrodiolides were synthesized through a convergent approach using an Evans aldol reaction, Keck esterification, and Yamaguchi macrolactonization, or Mitsunobu macrolactonization, as key steps. Moreover, introduction of an aminosugar to a macrodiolide aglycone by Schmidt glycosylation also afforded a new macrodiolide. Comparison between the conformation analysis of the macrolides, which we designed, and NMR analysis of the synthetic macrolides, indicated our stereoisomer library has significant diversity." @default.
- W1998377589 created "2016-06-24" @default.
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- W1998377589 date "2015-09-01" @default.
- W1998377589 modified "2023-10-18" @default.
- W1998377589 title "An architectonic macrolide library based on a C2-symmetric macrodiolide toward pharmaceutical compositions" @default.
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- W1998377589 doi "https://doi.org/10.1016/j.tet.2015.01.030" @default.
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