Matches in SemOpenAlex for { <https://semopenalex.org/work/W1998490246> ?p ?o ?g. }
Showing items 1 to 86 of
86
with 100 items per page.
- W1998490246 endingPage "428" @default.
- W1998490246 startingPage "423" @default.
- W1998490246 abstract "An analytical procedure is reported for the determination of rubidium in spent continuous ambulatory peritoneal dialysis (CAPD) fluids by flame and electrothermal atomic absorption spectrometry (FAAS, ETAAS). Samples of spent CAPD fluids were collected as 5 ml aliquots in polyethylene tubes and stored in a freezer at −20°C. Before analysis, samples were equilibrated to room temperature and analysed within 8 h. A total of 2 mg ml−1 of caesium was added to each sample and standard solution to overcome interferences from ionisation. An air–acetylene flame was applied in FAAS determinations. Analysis was performed against aqueous standards. The calibration graph was linear from 30.0 up to 5000 μg l−1 Rb, while the limit of detection (3 s) was found to be 20.0 μg l−1 rubidium. Good repeatability of measurement (RSD 1%) was obtained. Parameters were also optimised for determination of rubidium in spent CAPD fluids by ETAAS. Ten-fold diluted samples (3.5% nitric acid) were analysed applying standard addition calibration. The calibration graph was linear from 2.0 up to 30.0 μg l−1 rubidium, while the limit of detection (3 s) was found to be 1.0 μg l−1 rubidium (sample volume 10 μl). Good repeatability of measurement (RSD 5%) was obtained. The results of direct determination by FAAS and ETAAS were compared to those obtained after acid digestion of samples in Parr bombs. The accuracy of the procedure for direct determination was checked by spiking samples. In 73% of samples analysed, the differences between the results obtained by the two techniques, either for direct determinations of samples or for samples digested in a Parr bomb did not exceed ±10%." @default.
- W1998490246 created "2016-06-24" @default.
- W1998490246 creator A5038968746 @default.
- W1998490246 creator A5043082898 @default.
- W1998490246 creator A5051459295 @default.
- W1998490246 creator A5053771070 @default.
- W1998490246 date "1999-11-01" @default.
- W1998490246 modified "2023-09-23" @default.
- W1998490246 title "Optimisation of parameters for determination of rubidium in spent CAPD fluids by flame and electrothermal atomic absorption spectrometry" @default.
- W1998490246 cites W1819398518 @default.
- W1998490246 cites W1967031740 @default.
- W1998490246 cites W1975202693 @default.
- W1998490246 cites W1989626681 @default.
- W1998490246 cites W1994082639 @default.
- W1998490246 cites W1994210833 @default.
- W1998490246 cites W2015839361 @default.
- W1998490246 cites W2034168666 @default.
- W1998490246 cites W2041072355 @default.
- W1998490246 cites W2043185148 @default.
- W1998490246 cites W2046879292 @default.
- W1998490246 cites W2101395957 @default.
- W1998490246 cites W2332736226 @default.
- W1998490246 cites W2467454601 @default.
- W1998490246 doi "https://doi.org/10.1016/s0731-7085(99)00171-5" @default.
- W1998490246 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/10703999" @default.
- W1998490246 hasPublicationYear "1999" @default.
- W1998490246 type Work @default.
- W1998490246 sameAs 1998490246 @default.
- W1998490246 citedByCount "3" @default.
- W1998490246 crossrefType "journal-article" @default.
- W1998490246 hasAuthorship W1998490246A5038968746 @default.
- W1998490246 hasAuthorship W1998490246A5043082898 @default.
- W1998490246 hasAuthorship W1998490246A5051459295 @default.
- W1998490246 hasAuthorship W1998490246A5053771070 @default.
- W1998490246 hasConcept C113196181 @default.
- W1998490246 hasConcept C119128265 @default.
- W1998490246 hasConcept C121332964 @default.
- W1998490246 hasConcept C154020017 @default.
- W1998490246 hasConcept C178790620 @default.
- W1998490246 hasConcept C179104552 @default.
- W1998490246 hasConcept C185592680 @default.
- W1998490246 hasConcept C196765960 @default.
- W1998490246 hasConcept C23531484 @default.
- W1998490246 hasConcept C2778504605 @default.
- W1998490246 hasConcept C33619061 @default.
- W1998490246 hasConcept C43617362 @default.
- W1998490246 hasConcept C517785266 @default.
- W1998490246 hasConcept C526903357 @default.
- W1998490246 hasConcept C62520636 @default.
- W1998490246 hasConceptScore W1998490246C113196181 @default.
- W1998490246 hasConceptScore W1998490246C119128265 @default.
- W1998490246 hasConceptScore W1998490246C121332964 @default.
- W1998490246 hasConceptScore W1998490246C154020017 @default.
- W1998490246 hasConceptScore W1998490246C178790620 @default.
- W1998490246 hasConceptScore W1998490246C179104552 @default.
- W1998490246 hasConceptScore W1998490246C185592680 @default.
- W1998490246 hasConceptScore W1998490246C196765960 @default.
- W1998490246 hasConceptScore W1998490246C23531484 @default.
- W1998490246 hasConceptScore W1998490246C2778504605 @default.
- W1998490246 hasConceptScore W1998490246C33619061 @default.
- W1998490246 hasConceptScore W1998490246C43617362 @default.
- W1998490246 hasConceptScore W1998490246C517785266 @default.
- W1998490246 hasConceptScore W1998490246C526903357 @default.
- W1998490246 hasConceptScore W1998490246C62520636 @default.
- W1998490246 hasIssue "2" @default.
- W1998490246 hasLocation W19984902461 @default.
- W1998490246 hasLocation W19984902462 @default.
- W1998490246 hasOpenAccess W1998490246 @default.
- W1998490246 hasPrimaryLocation W19984902461 @default.
- W1998490246 hasRelatedWork W1998490246 @default.
- W1998490246 hasRelatedWork W2055701698 @default.
- W1998490246 hasRelatedWork W2061951347 @default.
- W1998490246 hasRelatedWork W2090435047 @default.
- W1998490246 hasRelatedWork W2333682883 @default.
- W1998490246 hasRelatedWork W2370199034 @default.
- W1998490246 hasRelatedWork W2802927235 @default.
- W1998490246 hasRelatedWork W3005427839 @default.
- W1998490246 hasRelatedWork W3114753283 @default.
- W1998490246 hasRelatedWork W3151535921 @default.
- W1998490246 hasVolume "21" @default.
- W1998490246 isParatext "false" @default.
- W1998490246 isRetracted "false" @default.
- W1998490246 magId "1998490246" @default.
- W1998490246 workType "article" @default.