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• W1998691109 abstract "High-temperature in situ x-ray measurements have been undertaken during the growth of Bi2Sr2Ca2Cu3O10+δ in order to determine the sequence of phases that form and the kinetics of growth. With a Ag-coated thin pellet of the starting mixture of Pb-doped Bi2Sr2Ca1Cu2O8+δ, Ca-cuprates, and CuO in an air atmosphere, major changes occur in the x-ray spectrum at temperatures as low as 790 °C. A triplet of lines associated with Ca2PbO4 forms as soon as the pellet reaches 790 °C and then disappears after 20 or 30 minutes. The Bi2Sr2Ca2Cu3O10+δ phase begins to grow at about 810 °C. For these rather porous pellets, about 20% of the sample transforms to Bi2Sr2Ca2Cu3O10+δ, as indicated by both x-ray intensities and superconducting magnetization studies." @default.
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• W1998691109 date "1995-07-01" @default.
• W1998691109 modified "2023-10-18" @default.
• W1998691109 title "Intermediate phases produced in growth of Bi₂Sr₂Ca₂Cu₃O_10+δ" @default.
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• W1998691109 doi "https://doi.org/10.1063/1.360610" @default.
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