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- W1998897789 abstract "Abstract Colloidal, monodisperse, single‐crystalline pyramidal CuInS 2 and rectangular AgInS 2 nanocrystals were successfully synthesized through a convenient and improved solvothermal process that uses hexadecylamine as a capping reagent. The crystal phase, morphology, crystal lattice, and chemical composition of the as‐prepared products were characterized by using X‐ray diffraction, transmission electron microscopy (TEM), high‐resolution TEM, and energy dispersive X‐ray spectroscopy. Results revealed that the as‐synthesized CuInS 2 colloid is in the tetragonal phase (size: 13–17 nm) and the AgInS 2 in the orthorhombic structure (size: 17±0.5 nm). A possible shape evolution and crystal growth mechanism has been suggested for the formation of pyramidal CuInS 2 and rectangular AgInS 2 colloids. Control experiments indicated that the morphology‐ and/or phase‐change of CuInS 2 and orthorhombic AgInS 2 colloids are temperature‐ and/or time‐dependent. CuInS 2 colloids absorb well in the range of visible light at room‐temperature, indicating its potential application as a solar absorber. Two photoluminescence (PL) subbands at 1.938 and 2.384 eV in the PL spectra of CuInS 2 colloids revealed that the recombination of the closest and the second closest donor–acceptor pairs within the CuInS 2 lattice, in which the donor defect (Cu i ) occupies an interstitial position and the acceptor defect (V In ) resides at an adjacent cation site. In addition, the synthesis strategy developed in this study is convenient and inexpensive, and could also be used as a general process for the synthesis of other pure or doped ternary chalcogenides that require a controlled size (or shape). This process could be extended to the synthesis of other functional nanomaterials." @default.
- W1998897789 created "2016-06-24" @default.
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- W1998897789 date "2007-10-18" @default.
- W1998897789 modified "2023-10-17" @default.
- W1998897789 title "Shape- and Phase-Controlled Synthesis of Monodisperse, Single-Crystalline Ternary Chalcogenide Colloids through a Convenient Solution Synthesis Strategy" @default.
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- W1998897789 doi "https://doi.org/10.1002/chem.200700618" @default.
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