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- W1998918133 abstract "A general method for the preparation of dioxotungsten(VI) complexes of the type [WO2L(MeOH)] (where LH2 = the Schiff’s base derived from salicylaldehyde or o-vanillin and benzoylhydrazide, salicylhydrazide, furoylhydrazide, and isonicotinoylhydrazide) using [WO2(acac)2] (acacH = acetylacetone) as a precursor, is described. These complexes have been characterized by elemental analysis, electrical conductance, IR, electronic, and NMR spectral, electrochemical, and magnetic susceptibility measurements. The structure of [WO2(o-C6H4CH=NN=C(O)C6H5)(MeOH)]·MeOH (1a·MeOH) has been determined by single-crystal X-ray diffraction analysis. 1a·MeOH crystallizes in the space group Pbc21 with a = 6.992(2), b = 16.190(2), c = 31.390(4) A, V = 3553.4(12) A3, Z = 8, RF = 0.050, and Rw = 0.054. The tungsten atom has a highly distorted octahedral coordination in which anionic oxygen atoms of the tridentate ligand are mutually trans and are cis to the cis-dioxo group." @default.
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- W1998918133 date "1995-10-01" @default.
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- W1998918133 title "Dioxotungsten(VI) Complexes of ONO Donor Ligands and the X-Ray Crystal Structure of [WO<sub>2</sub>(<i>o</i>-OC<sub>6</sub>H<sub>4</sub>CH=NN=C(O)C<sub>6</sub>H<sub>5</sub>)(MeOH)]·MeOH" @default.
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- W1998918133 doi "https://doi.org/10.1246/bcsj.68.2847" @default.
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